Artisan Technology Group Quest 210 Specifications Page 32
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Reaction Vessels
Reaction
Vessels
Reaction Vessels
Each side of the Reactor Unit contains a reaction vessel bank where
10
vessels can be
mounted, for a total of
20
synthesis positions. The reaction vessels are clear Teflon
tubes, and are disposable
-
intended for one time use.
A
frit is pre-installed in the bottom
of each reaction vessel. The reaction vessels are available in either
5
or
10
rnL
sizes.
Above each reaction vessel bank is the Upper Manifold, which contains fluidic
pathways which access the reaction vessels. Located below the reaction vessel bank is
the Lower Manifold, which is used to control reaction vessel draining. Both manifolds
have male fittings over which press into the Teflon Reaction vessels. By lowering the
Upper Manifold over the bank of RVs, the
rv
tube ends press over the male fittings of
both upper and lower manifolds, creating a leak-tight seal for the reaction vessels.
Frit
The frit is a teflon filter that is installed in the bottom of each reaction vessel. The frit
allows for draining of solution from the reaction vessels while containing the solid
support resin within the vessel.
Heating and Cooling
NOTE Reaction Temperature parameters may be set using the Control Unit display
and keypad. For instructions on setting the temperature parameters, see Operating the
Quest
210,
Temperature Control.
Heating and Cooling Block
The heatinglcooling blocks are aluminum plates mounted behind the reaction vessel
holders on each side of the instrument. When RVs are mounted on the instrument they
are in contact with the heater block.
Heat is provided by a resistive heater mounted inside the heater block. Cooling is
accomplished by using a recirculating chiller to flow cold liquid (such as ethanol)
through a channel mounted at the rear of the heater block. Each reaction vessel bank on
the Quest, (Side
A
and Side
B)
can be set to two independent temperatures.
QUEST
210
User
Manual
Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com
- 1
- Manual Synthesizer 2
- Table of Contents 4
- Specifications 7
- Symbols 8
- User Supplied ltems 9
- Limited Warranty Agreement 10
- EXCLUSIONS 11
- IS NOT COVERED) 11
- SITE PREPARATION 12
- INSTALLATION 12
- Immunity Information 13
- Maintenance 14
- Contact Information 15
- Overview 17
- Quest Installation Procedure 19
- Installation Procedure 20
- Introduction 21
- Umbilicus Connections 21
- Procedure 22
- Solvent 24
- Install the Glass Waste Tank 27
- Connect Power to the Unit 28
- Install a 4L Solvent Bottle 28
- System Overview 30
- Reactor 31
- Reaction 32
- Heating and Cooling 32
- Manifold 34
- Manifold Control Valves 35
- Metered Gas Needle Valve 36
- Utility Ports 36
- WARNING Always place the 37
- Waste Tray and Container 39
- Sample Collection 39
- Collection Racks 39
- Controller Unit 40
- Screen and Keypad 41
- Mode Button 42
- Forward and Back Buttons 42
- Parameter Setting Buttons 42
- Controller 43
- System Gas 44
- Electrical Outlet 44
- Power Switch 44
- Operating the Quest 46
- Remove Old Reaction Vessels 47
- Reaction Vessels 48
- Temperature 50
- 5mL 5mL 50
- Repeat this 52
- WARNING 53
- Starting a Reaction 55
- MixEvery 56
- Agitating 56
- Operating the 57
- NOTE The agitator needle 58
- Temperature Control 59
- 3/32" 61
- Parallel Solvent Addition 63
- Changing 67
- Solvent Bottle 67
- Quest 210 69
- Providing 70
- Collection Rack Options 71
- Troubleshooting 76
- Glossary 78
- Appendix 82
- Control Box 82
- Display Screens 82
- Quest Controller Box and 83
- Display 83
- Sign-on Screen 84
- Firmware Version Screen 85
- Agitation Control Screen 86
- FORWARD/BACK 87
- Set Temperature Screen 88
- Monitor Temperature Screen 89
- Other Functions Screen 90
- Results 91
- ERWARDIBACK 92
- Self Test Screen 93
- Heaters screen appears 94
- Starts/Stops agitation 94
- Restore Defaults Screen 95
- StartEtop Heaters 96
- Plumbing Schematic 97
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