Artisan Technology Group Quest 210 Specifications download pdf (Page 20)

Addition of Reagent Under Nitrogen to the Reaction Vessels

Adjust the Metered Gas Needle Valve located on the top of the Quest Reactor Unit

until you see a steady stream of gas bubbling through the oil bubbler when one of the

Luer Plugs is removed from the Upper Manifold.

Using a syringe add the alcohol or carbonyl diversity reagent in

NMP

to each

RV.

a. Remove the Luer Plug from the first RV Luer Port (twist and pull) and insert the

syringe needle below the Teflon lines of the male Teflon

fitting. Take care

not to score the interior surfaces of the Luer Port with the needle. Marring the

surface can affect the sealing of the Luer Port.

b. Dispense

mL of

-2-methoxybenzoy1)-2-pyrrolidinemethanol

in NMP to the

first RV.

Replace the Luer Plug (twist and push) onto the Upper Manifold.

d. Add the appropriate alcohol or carbonyl solution in NMP to the remaining

RVs

in the same manner as the first as described in

Table

Using a syringe, add

mL of catalyst solution in NMP to each RV in the same

manner as the alcohol and carbonyl diversity reagent (steps 1 and 2a-2d above).

Blanket RVs with nitrogen by turning the

left

Manifold Control Valve to "CLOSED".

Then, turn the

right

Manifold Control Valve to "CLOSED.

Drain Gas Metered Gas

Utility

Drain Gas

Utility

Metered Gas

Utility 1 Utility

Toggle the "Upper Manifold Membrane" switch to "CLOSED". Please refer to the

Quest User Manual for the function of the Upper Manifold Membrane Switch.

Adjusting the Agitation Bar

Raise the Agitation Bar up by pushing the Agitation UP soft key located to the right

of the Quest Controller Unit display.

Use the

7/64"

hex wrench supplied with the Quest to loosen the Agitation Stops.

Adjust the Agitation Stops on the Reactor Unit so the maximum magnet height is

-2

cm below the solvent level in the RVs. Tighten the Agitation Stops so both stops are

at the same height.

Argonaut Technologies

Part

Number

102298

04/02/98

Quest Tutorial

Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com

1 2 ... 15 16 17 18 19 20 21 22 23 24 25 ... 37 38

Comments to this Manuals

No comments

Artisan Technology Group Quest 210 Specifications Page 20

Comments to this Manuals

Related products and manuals for Synthesizer Artisan Technology Group Quest 210