Artisan Technology Group Quest 210 Specifications download pdf (Page 29)

Sample

Work

Using a Savant SpeedVac (Model SS620DDA SpeedVac or equivalent), evaporate

the solvent from the 20 mL scintillation vials containing the product.

Re-weigh the scintillation vials and calculate the product mass yields using the

weights determined earlier.

Add

THF

to each scintillation vial, mix to dissolve the products, and analyze

Gas Chromatography for product purity

(Table

4).

Theoretical

Yield

Purity

Alcohol Product

pyrrolidinemethanol

epiandrosterone

18.5

rng

69%

Table

Alcoholysis and Carbonyl Hydrosilylation of PS-DES resin

yield

calculated based on a resin loading of

0.68

mmolelg)

Argonaut Technologies

Part

Number 102298

04102198

Quest Tutorial

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Artisan Technology Group Quest 210 Specifications Page 29