I
AlcohollCarbonyl
AlcohoVCarbonyl Structure Amount
1
1
-naphthaleneethanol 206
mgl
4
rnL
NMP
2.2-diphenylethanol
Ph
238
mgl
ho
H
4
rnL
NMP
Ph
218
mgl
4
rnL
NMP
I
Table
3.
Preparation of Alcohol and Carbonyl Solutions in Anhydrous NMP
(0.3
M)
B.
Instrument Preparation
Before proceeding, prepare the appropriate alcohol/carbonyl and catalyst solutions
needed for the tutorial. The alcohols, carbonyls, and catalyst may take some time to
dissolve and should therefore be prepared at least an hour before they are needed for the
experiment.
CAUTION:
Always wear gloves, eye protection, and proper clothing such as a lab
coat when working with the Quest.
Prior to Starting the Synthesis:
Read the Quest
2
10
User Manual.
Verify that the Quest was installed according to the Quest Installation Procedure
found in the Quest
2
10
User Manual.
Verify that a
30-40
psi inert gas supply is connected to the Quest Controller Unit.
Flush tetrahydrohan
(THF)
through the Upper Manifold of the Quest by performing
several solvent fills and drains (see Chapter
3
of the Quest User Manual).
Familiarize yourself with the nomenclature and various components of the Quest
Reactor
Unit
(Figure
2).
Argonaut Technologies
Part Number 102298
04/02/98
Quest
Tutorial
Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com
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