Artisan Technology Group Quest 210 Specifications download pdf (Page 2)

ARGONAUT

TECHNOLOGIES

Quest

User

Tutorial

R'OH or

SLEt

PS-DES

(6equiv

mol% RhCI(PPh3)3

NMP

mL), 60°C,

50 mg, ArgoCap)

0.4

HFIpyridine in THF

mL)

2) MeOSiMe3

(0.5 mL,

2 equiv. relative to

Figure

Synthesis of Resin Bound Ethers to Form the Corresponding Alcohol

The objective of the Quest

10 Organic Synthesizer Tutorial is to introduce and

familiarize new users to the instrument. The tutorial guides the user through instrument

operations using a synthesis as a training vehicle. The reaction scheme for the synthesis

is shown in Figure

All of the materials necessary for the Quest 21 0 User Tutorial are

listed in Table

Please allow for extra materials so there is plenty of reagent and

solvent available for performing the syntheses.

The tutorial is divided into the following sections, (I) Instrument and Solution

Preparation,

(11) Coupling Reaction, (111) Addition of CleavageIScavenger and Product

Collection, (IV) Cleaning and Maintenance and Sample Work UpIAnalysis. The

experiment is performed in duplicate using a bank of ten reaction vessels (RVs) on the

Argonaut Technologies

Part

Number 102298

04/02/98

Quest Tutorial

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Artisan Technology Group Quest 210 Specifications Page 2